Automated multipurpose xray diffractometer instruction. Any evidence that may be obtained can help in a particular situation. Expand the file to see the data file that needs to be deleted. Xray diffraction measurements are taken on a rigaku smartlab diffractometer using cuk. Before using the product, read the safety precautions in handling xray equipment found in the smartlab automated multipurpose xray diffractometer instruction manual me1157111573. The box between the tube and cbo unit is ge 111 monochrometer. European smartlab applications workshop anka the synchrotron radiation facility at kit thursday, february 27 and friday, february 28, 2014 rigaku is organizing a 2day workshop around the versatile smartlab. Polytec msa500 micro system analyzer vibrometer anton paar afm. Rigaku presents latest xray diffraction instrumentation. Source standard copper anode sealed tube source with tungsten filament. Rigaku smartlab xray diffractometer the rigaku smartlab is the state of the art in highly automated, fully modular, multipurpose xray diffractometer.
Perhaps its most novel feature is the new smartlab studio ii software, which. Sample name and memo should contain some information about the data, minimally duplicating. Area max will open your file folder and it will look similar to the following image. It is capable of performing most common xrd measurements as well as many uncommon ones, and can be rapidly switched between various optical. Automated multipurpose xray diffractometer 1 overview smartlab, automated multi purpose xray diffractometer, is an xray diffraction system equipped with a highaccuracy thetatheta. Rigaku smartlab osus cemas the ohio state university.
Fast data collection is enabled by a 9 kw rotating anode source which produces a high flux of xray intensity. In addition, it has an inplane arm axis which rotates the counter around the axis perpendicular to the axis of 2 rotation, effectively pulling the counter to the front allowing both inplane and outofplane grazing incident diffraction gid for thin films. The login name for the software is administrator and there is no password for the. The file will open and display the image scanned from the image plate. The rigaku smartlab is a multipurpose xrd which can switch between focusing bragg brentano, bb and parallel beam pb geometries. As with the bruker, the xray source is a copper sealed tube target producing cu k.
Schedule online in cypoint for equipment use and sign logbook for each experiment. Rigaku introduces new dualwavelength rotating anode xray diffractometer. Rigaku workshop smartlab applications 1718 september 20 2nd announcement rigaku are pleased to inform you that we will organize 2day workshop on smartlab xray diffractometer at the rutherford. Rigaku smartlab is the newest and most novel highresolution xray diffractometer xrd available today. Any explorations are strongly prohibited unless permitted. The rigaku smartlab xray diffraction system xrd is a fully automated, modular system for advanced xray diffraction measurements on a wide range of materials including thin films and powders.
Combined xrd and saxs analysis of nanomagnetic materials. Rigaku smartlab west campus materials characterization core. If the names of the data files are unknown, access the detailed file list given in the file manager in the rigaku. Rigaku ultima iv powder diffractometer operation summary 11292012 a.
The rigaku smartlab xray diffractometer located in lab 3510 in the engineering building is operated by the zevalkink research group. Never surf the web on the xps computer to minimize the risk of the computer being. Input is a rigaku format file see guide for more info. Now, i found that the format of rigaku img file changes according to the type of instruments. Forensic science is deeply involved with solving the unknown. Rigaku introduces new central software platform that. Rigaku introduces newest smartlab intelligent xray. Smartlab toys downloadable pdf product instructions. Rigaku hypix3000 rigaku hypix6000 technology hybrid pixel array hybrid pixel array size 238. Xrd rigaku smartlab microelectronics research center.
On the rigaku dmaxb instrument computer, using windows explorer, navigate to the data file directory c. Phase identification of a forensic sample rigaku global website. Does anyone know how to convert the xray diffraction data by. Smartlab the smartlab is the most novel highresolution xray diffractometer available today. The software can read img files by fuji and hamamatsu but rigaku img file is not supported. Now your integrated data rint ascii file is saved under z. Rigaku ultima iv powder diffractometer operation summary 11.
In no event will rigaku corporation be responsible for the results of the use of this manual. Featured at the exhibition is the new nextgeneration. Cornell center for materials research rigaku smartlab xray. Components and specifications i names of parts hypix400 main 111dit dhypix400 main unit a hybrid multidimensional pixel detector hypix400 mount holder. Rigaku smartlab xrd shared equipment authority rice. Among the equipment is rigaku smartlab xray diffraction system allows for multiple types of analysis using the following available techniques. Insert glass sample holder in upper part of the stage. If you cannot see any spots or rings, the intensity scale is probably off. Click measurement conditions and set parameters such as start and stop angle, and also scan speed measured in degreesmin. File name is the full path to the where the file will be saved.
Figure 1 shows the smartlab goniometer equipped with a 9 kw rotating anode generator, refl ection sample stage and dtex ultra 250 1d silicon strip detector. I am having difficulty to open rigaku raw file into eva. Rigaku corporation has announced the release of the new nextgeneration rigaku smartlab intelligent multipurpose xray diffractometer. Rigaku smartlab xrd 1 yale west campus materials characterization core please follow the sop strictly to keep the facility in good condition. Standard operating procedure for the rigaku smartlab xrd. Automated multipu rpose xray diffractometer 1 overview smartlab, automated multi purpose xray diffractometer, is a thin film analysis system equipped with a highaccuracy thetatheta. This system is ideal for either powder measurements braggbrentano geometry or for thin film measurements parallel beam geometry. Central facility for xray materials characterization. As a rule, only one set of instruction manual is supplied for each. This software package was designed to easily guide the user through all the steps necessary to run. Continuouswave and nanotomicrosecond timeresolved photoluminescence pl.
Xray diffraction system singleelement bragg brentano powder and parallel beam single crystal incident beam optics highpower 9kw xray source for faster acquisition times, thin samples 1d silicon strip xray detector for fast, mediumresolution rsms and pole figures inplane diffraction goniometer for ultra thin and 2d materials. The workshop focuses on application and operation on the. Full article xrd application note measurement of microscopic regions using a highspeed 2dimensional detectorevaluation of microscopic regions of carbide tools rigaku. Start up the smartlab guidance in the smartlab control pc. Schedule online in cypoint for equipment use and sign. Rigaku may change the specifications of the software product and the contents of the printed materials including the manual without notice in the future. Open rigaku smart lab guidance software from the desktop of the system. The rigaku smartlab has a new technology that allows both focusing geometry and parallel beam geometry without changing optical components.
Rigaku workshop smartlab applications 1718 september 20 2nd announcement rigaku are pleased to inform you that we will organize 2day workshop on smartlab xray diffractometer at the rutherford appleton laboratories, oxford, uk on september 17th and 18th 20. This training allows you to do a basic xray scan using braggbrentano bb or parallel beam pb focusing. Rigaku smartlab intelligent multipurpose xray diffractometer. A 2d detector makes it possible to analyze texturing on polycrystalline samples.
Rigaku a global leader in xray analytical instrumentation is an exhibitor and. May 19, 2020 no special effort was made to control the preferred orientation in the grains. Advanced stateoftheart highresolution xrd system powered by guidance expert system software. Issue 82 of the bridge, the materials science newsletter from rigaku, is now online. Interchangeable stages and optical components permit a large range of xray techniques to be performed on this instrument. Pdxl software based refinement to obtain lattice parameters, unit. Rigaku xrdsystem instruction manual v41903 the krishnan. Issue 66 of the bridge, the materials science newsletter. Finding the peak position, you need to provide a starting angle, where you expect to find a peak to find. Rigaku smartlab massachusetts institute of technology.
Smartlab has many unique features for application categories mentioned above. Rigaku smartlab is the newest and most novel highresolution xray diffractometer xrd. Perhaps its most novel feature is the new smartlab studio ii software, which provides the user. The data collection program for the smartlab is called smartlab guidance. If youve misplaced your product instructions, just click a link below to download a pdf version. The smartlab guidance reference manual this manual describes the basic functions and operations of smartlab guidance, the control software of smartlab. Is there a manual from which i can understand the file format. Powder diffraction reflectivity intermediate resolution reciprocal space mapping high resolution user. Perhaps its most novel feature is the smartlab guidance software, which provides you with an. Sample name has a 30 character size limit for most displays of data. The rigaku smartlab is a multipurpose diffractometer with a wide variety of optics and sample stages that are available. Completion of rigaku smartlab xrd user registration form is required after the in person training. Automatic identification of crystal structure with pdf database.
Smartlab system equipped with an inplane axis and a 2d detector. Thermogravimetric analysis tga is located in room 2423 calit2 building building 325 on uci campus map thermogravimetric analysis tga is a method of thermal analysis in which the mass of a. Rigaku 9009 new trails drive the woodlands, tx 77381 2862230 modified 06142012 table of contents. The system uses a high power, 9 kw rotating anode xray generator which allows faster collection times with less background noise and is optimized for. Click use another account, and then enter rigaku in the username box without a password.
Perhaps its most novel feature is the smartlab guidance software, which provides you with an intelligent interface that guides you through the intricacies of each experiment. If no peak is found, it may be that the width is unusual and you can. Xrd characterization of refractory powders by search. The experimental patterns were compared with the diffraction scans of pure compounds maintained in the icdd powder diffraction file pdf. Aug 05, 20 for the love of physics walter lewin may 16, 2011 duration. Thermal, elemental, mechanical, physical and rheological properties. Left side is incident optics, central part is sample stage, right side is detector side optics. It generates high intensity xrays with a wavelength of 1. Completion of rigaku smartlab xrd user registration form is required after the inperson training. This manual describes the correct use of the product as well the usage precautions to be observed. At all times safety is paramount in using this instrument. Rigaku smartlab multipurpose diffractometer rigaku crsource powder diffractometer bruker d8 with gadds 2dimensional detector other instruments bruker d8 hrxrd bruker handheld xrf. In the presentation, details of xrd solutions with comprehensive examples demonstrated by rigakus xrd product lineup including the above mentioned smartlab will be discussed.
Yamano, rigaku corporation, japan this months issue contains a rigaku journal article describing xrd analysis of modern functional thin films using a 2dimensional detector on the rigaku smartlab. It is capable of performing most common xrd measurements as well as many uncommon ones, and can be rapidly switched between various optical configurations including both braggbrentano and parallelbeam geometries. Or any software or module which can be used to read the. Perhaps its most novel feature is the new smartlab studio ii software, which provides the user with an intelligent user guidance expert system functionality that guides the operator through the intricacies of each experiment. Data analysis for the data analysis using jade program, the data you saved on z. The rigaku smartlab is our swiss army knife of tools. The woodlands, texas prweb december 27, 2018 the december 2018 edition of the bridge, the materials science newsletter from rigaku corporation, is now available online on the. Uvvis absorption measurements are performed on an agilent cary 5000 spectrophotometer. Jul 23, 20 rigaku corporation is pleased to announce a new software product, smartstudio, which acts as a centralized command center for operating rigakus top of the line smartlab xray diffractometer, as well as carrying out all of the postmeasurement analysis calculations from a centralized user interface. View source for rigaku smartlab xray diffraction system. Confirm that the following window appears on the desktop, indicating that the hypix server software is running. Select the file name of the xray run you just performed, probably the last item in the list.
1107 240 1444 589 1036 844 130 629 1034 309 559 812 1453 1274 1426 70 940 253 1403 1129 524 707 333 339 1019 293 1153 855 674 416 184 185 29